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  <front>
    <journal-meta />
    <article-meta>
      <title-group>
        <article-title>Numerical and Experimental Analysis in Endodontic Rotary Files Under Cyclic Fatigue or Torsional Stress</article-title>
      </title-group>
      <contrib-group>
        <contrib contrib-type="author">
          <string-name>Damiano Alizzio</string-name>
          <email>damiano.alizzio@unime.it</email>
          <xref ref-type="aff" rid="aff2">2</xref>
          <xref ref-type="aff" rid="aff3">3</xref>
        </contrib>
        <contrib contrib-type="author">
          <string-name>Fabio Lo Savio</string-name>
          <email>flosavio@diim.unict.it</email>
          <xref ref-type="aff" rid="aff1">1</xref>
          <xref ref-type="aff" rid="aff3">3</xref>
        </contrib>
        <contrib contrib-type="author">
          <string-name>Marco Bonfanti</string-name>
          <email>bonfa.marco@tiscali.it</email>
          <xref ref-type="aff" rid="aff0">0</xref>
          <xref ref-type="aff" rid="aff3">3</xref>
        </contrib>
        <aff id="aff0">
          <label>0</label>
          <institution>Department of Electrical, Electronic and Computer Engineering, University of Catania</institution>
          ,
          <addr-line>Catania, CT</addr-line>
          ,
          <country country="IT">Italy</country>
        </aff>
        <aff id="aff1">
          <label>1</label>
          <institution>Dip. di Ing. Civile e Architettura, Università di Catania</institution>
          ,
          <addr-line>Catania, CT</addr-line>
          ,
          <country country="IT">Italy</country>
        </aff>
        <aff id="aff2">
          <label>2</label>
          <institution>Dip. di Ingegneria, Università degli Studi di Messina</institution>
          ,
          <addr-line>C.da Di Dio, 98166 Sant'Agata, Messina</addr-line>
          ,
          <country country="IT">Italy</country>
        </aff>
        <aff id="aff3">
          <label>3</label>
          <institution>ICYRIME 2020: International Conference for Young Researchers in Informatics, Mathematics, and Engineering</institution>
          ,
          <addr-line>Online</addr-line>
        </aff>
      </contrib-group>
      <fpage>59</fpage>
      <lpage>65</lpage>
      <abstract>
        <p>This study aims to analyze the mechanical behavior of two types of rotating endodontic instruments with diferent cross sections, both made by Coltene (Hyflex CM 40.04 of NiTi alloy and Hyflex EDM 40.04 of Heat-treated NiTi alloy), under cyclic fatigue or torsion. The study of the mechanical behavior combined the traditional approach, consisting in experimental investigations, with a finite element analysis under similar bending and torque conditions. The non-linear superelastic behavior of the NiTi alloy for fatigue and torsion, derived from experimental tests based on models in the scientific literature, was applied to the numerical analysis. A thermographic investigation was associated with the usual mechanical experimental tests to assess the dependence of the temperature on the deformations undergone by the endodontic files under stress, especially near the breakage. The comparison between experimental and numerical results was in good agreement for both types of files analyzed.</p>
      </abstract>
      <kwd-group>
        <kwd>eol&gt;Endodontic Instruments</kwd>
        <kwd>FEA</kwd>
        <kwd>Cyclic Fatigue</kwd>
        <kwd>Torsion</kwd>
        <kwd>Thermography</kwd>
      </kwd-group>
    </article-meta>
  </front>
  <body>
    <sec id="sec-1">
      <title>1. Introduction</title>
      <p>cycles.</p>
      <p>
        Instead, the torsional failure is characterized by a
In endodontic therapy, rotary files made of nickel-tita- maximum torsional load and a critical angle of
rotanium alloy (NiTi) are widely used when processing tion. This reveals the capability of the file to twist
bethe root canal. This is due to the superelasticity and fore fracture [
        <xref ref-type="bibr" rid="ref10">10</xref>
        ].
shape memory characteristics of NiTi, which allow it Diferences in cyclic-bending or torsional strength
to produce desirable tapered shapes while maintaining between various NiTi endodontic instruments depend
lfexibility and strength when rotating within curved on the diferent geometries and manufacturing
techcanals [
        <xref ref-type="bibr" rid="ref1">1</xref>
        ]. The shape memory of NiTi alloys derives niques, such as heat treatment, machining, and surface
from a reversible solid-state phase transformation be- treatments [
        <xref ref-type="bibr" rid="ref11 ref12 ref5 ref6 ref7">5, 6, 7, 11, 12</xref>
        ].
tween the austenitic and martensitic structures, known An alternative to experimental investigations is
repas “thermoplastic martensitic transformation” [
        <xref ref-type="bibr" rid="ref2">2</xref>
        ]. resented by a numerical method that allows
analyz
      </p>
      <p>
        Therefore, the NiTi alloy is able to recover its orig- ing the mechanical behavior of endodontic files: the
inal shape under a range of high deformations. How- Finite Element Analysis (FEA) [
        <xref ref-type="bibr" rid="ref13">13</xref>
        ]. FEA calculates
ever, NiTi rotary instruments have a high risk of frac- stress distributions on files for assigned geometries,
ture during clinical operation [
        <xref ref-type="bibr" rid="ref3">3</xref>
        ]. Many variables might material properties and loading conditions, before
procontribute to the file failure, but the two main causes totyping [
        <xref ref-type="bibr" rid="ref14 ref15">14, 15, 16, 17, 18</xref>
        ].
are cyclic fatigue and torsional stress [
        <xref ref-type="bibr" rid="ref4 ref5 ref6 ref7 ref8">4, 5, 6, 7, 8</xref>
        ]. The purpose of this study is to perform a FEA on
Cyclic fatigue seems to be more prevalent in curved two types of endodontic files having diferent
crossroot canals, whereas torsional failure might occur even section geometries (Hyflex CM 40.04 and Hyflex EDM
in a straight canal [
        <xref ref-type="bibr" rid="ref9">9</xref>
        ]. When NiTi rotary instruments 40.04 both made by Coltene/Whaledent AG,
Altstatare loaded in a cyclic mode, they will undergo both ten, Switzerland), subjected to bending cyclic fatigue
tensile and compressive stress in curved canals. This or torsional stress. FEA results will be validated by
excould cause fatigue failure after a certain number of perimental tests.
      </p>
    </sec>
    <sec id="sec-2">
      <title>2. Materials and Methods</title>
      <sec id="sec-2-1">
        <title>The endodontic instruments object of this study are very diferent in terms of geometrical and constructive characteristics. EDM 40.04 has a highly variable</title>
        <p>
          Cyclic fatigue test results: mean ± SD of static bending force; number of rotations, dynamic bending and temperature of
the hotspot in middle of curvature at breakage. Courtesy of the authors [
          <xref ref-type="bibr" rid="ref7">7</xref>
          ].
Torsional test results: mean ± SD of static bending force; number of rotations, dynamic bending and temperature of the
hotspot at breakage.
        </p>
        <p>Instrument</p>
        <p>Angle of breakage</p>
        <p>Torque at breakage</p>
        <p>Time to breakage</p>
        <p>Temperature of hotspot at breakage
EDM 40.04
CM 40.04
376.32 ± 20.25 1.080 ± 0.052 31.365 ± 0.442 32.7 ± 1.3
241.44 ± 12.15 1.364 ± 0.29 20.127 ± 0.123 31.4 ± 0.2
Diferent superscript letters in the same column show statistically significant diference (  &gt; 0.05)
[deg]
computing was adopted for both the two types of
excitation. The geometrical shape of both rotary file types
was replicated in CAD environment starting from
microtomographic detections on relative commercial
products.</p>
        <p>Meshes of the CAD models were made according
to the Voronoi-Delaunay algorithm with 16 Jacobian
points per element.</p>
      </sec>
    </sec>
    <sec id="sec-3">
      <title>4. FEA on cyclic fatigue tested samples</title>
      <p>analysis was implemented setting up a four-event cyclic
calculation starting from the bending analysis
previously described. The fatigue analysis leaded back to
the meshes relative to the bending analysis. Moreover,
each event was set as an impulsive load (R = 0) and and 8.841 for EDM 40.04, as a confirmation of the good
imposed on the mesh model. The number of cycles re- quality of the models. Boundary conditions were
apported agreements with the experimental tests. In fact, plied with a fixed constraint on the cutter surfaces
relthe damage diagrams for both the models indicated a ative to the grip (5 mm from the file tip) and a hinge
nodal distribution at 100% of material damage at 1,490 joint constraint to the file stem. Remote time-dependent
cycles for CM 40.04 and 1,840 cycles for EDM 40.04, displacements through rigid beams were applied to the
respectively (Fig. 9). last cross-section of the stem, at the drive connection,
in order to simulate the torsion deformation. These
displacements were consisted in a revolution of the
5. FEA on cyclic fatigue tested ultimate stem cross- section relative to the rotating
samples driver around the file axis. Deformations were
progressively applied with a linear time dependence to
The mesh of CM 40.04 counted 42,897 nodes and 27,163 ensure a rotational velocity simulation of 2 rpm for
tetrahedral elements (element size of 0.12 ± 0.005 mm), both the models. Results confirmed compliance with
while that of EDM 40.04 consisted of 42,336 nodes and the model of the material constitutive curve.
Simu26,809 tetrahedral elements (element size of 0.15 ± 0.01 lated time-to- failure durations returned strain values
mm). The maximum Jacobian ratio was 4.98 for CM of 22.11 s for CM 40.04 and 30.55 s for EDM 40.04,
rela40.04 and 7.21 for EDM 40.04, respectively. The max- tive to failure angles equal to 265.32 for CM 40.04 and
imum aspect ratio returned was 10.306 for CM 40.04 366.624 EDM 40.04, respectively. It has to be noted
how the breakage location was well predictable and
recognized on both the models (Fig. 10). Analysis
returned that the most stressed zone was computed at
0.93 mm from the grip for CM 40.04 and at 0.29 mm
from the grip for EDM 40.04. Moreover, stress-strain
curves relative to the most stressed element were
extrapolated from the FEA. Figures 11a,b show the
simulated phase transformation for rotation and strain of
the most stressed element, respectively. It is clear that
the failure occurs in the martensite phase for both the
models.</p>
    </sec>
    <sec id="sec-4">
      <title>6. Results and Conclusion</title>
      <sec id="sec-4-1">
        <title>An accurate numerical simulation and experimental</title>
        <p>tests on two diferent rotary endodontic files were
performed in order to analyse both the cyclic fatigue and
torsional behaviour. Simultaneous thermographic
investigation was a helpful element of validation of
results.</p>
      </sec>
    </sec>
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