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  <front>
    <journal-meta>
      <journal-title-group>
        <journal-title>ITEA-</journal-title>
      </journal-title-group>
    </journal-meta>
    <article-meta>
      <title-group>
        <article-title>Automation of programmed laboratory equipment and development of a virtual device for measuring imitance based on graphic LabVIEW</article-title>
      </title-group>
      <contrib-group>
        <contrib contrib-type="author">
          <string-name>Igor-Mykhailo Midyk</string-name>
          <xref ref-type="aff" rid="aff1">1</xref>
        </contrib>
        <contrib contrib-type="author">
          <string-name>Olha Lysa</string-name>
          <xref ref-type="aff" rid="aff0">0</xref>
        </contrib>
        <aff id="aff0">
          <label>0</label>
          <institution>Lviv National Agrarian University</institution>
          ,
          <addr-line>1, V.Velykoho str., Dubliany-Lviv, 80381</addr-line>
          ,
          <country country="UA">Ukraine</country>
        </aff>
        <aff id="aff1">
          <label>1</label>
          <institution>National University “Lviv Polytechnica”</institution>
          ,
          <addr-line>12, S. Bandera str., 79013, Lviv</addr-line>
          ,
          <country country="UA">Ukraine</country>
        </aff>
      </contrib-group>
      <pub-date>
        <year>2021</year>
      </pub-date>
      <volume>1</volume>
      <fpage>6</fpage>
      <lpage>8</lpage>
      <abstract>
        <p>A virtual measuring instrument based on the LabVIEW hardware and software platform and a compatible NI USB 6009 unit has been proposed, developed and implemented for imitation control of vegetable juice quality indicators. A sinusoidal test signal in the form of alternating voltage with amplitude 10-20 mV. A structure has been developed that allows switching to the desired type of measurement, based on fixed instantaneous values of voltage and current of the conductometric cell, ie on measurements of rms voltage, measurements of rms current, module measurements, measurements of active and reactive components. A virtual device consisting of a personal computer with LabVIEW software, a NI USB 6009 unit and a juice conductivity cell was used to determine the content of heavy metals in this juice. In the same way, in production conditions at low cost, you can quickly control the quality of vegetables from which the juice is obtained.</p>
      </abstract>
      <kwd-group>
        <kwd>1 Immittance</kwd>
        <kwd>conductometric cell</kwd>
        <kwd>virtual tool</kwd>
        <kwd>rms value</kwd>
        <kwd>LabVIEW</kwd>
      </kwd-group>
    </article-meta>
  </front>
  <body>
    <sec id="sec-1">
      <title>1. Introduction</title>
      <p>Agricultural products, in particular vegetables, are an important component of Ukraine's export
potential. Vegetables are a source of nutrients, including carbohydrates, fiber, protein, organic acids, as
well as vitamins and minerals. Thanks to these substances and their compounds, vegetables have
antioxidant, antibacterial, antifungal, antiviral and anticancer properties. However, at the same time,
vegetables can contain toxins, nitrates and other harmful elements, which, depending on their content,
are dangerous to human health, impair taste and nutritional value. Therefore, it is important to identify
and quantify the useful and harmful elements present in vegetables. The task of quantitative assessment
of useful and harmful elements in vegetables is becoming even more urgent, as the world markets have
much stricter requirements for product quality. This brings to the fore a number of issues related to the
development of rapid methods for assessing the quality and safety of products, with the development
of a tool for studying the quality of vegetable products.</p>
      <p>As it is important to produce safe food products, free, in particular, from heavy toxic metals, the
development of a virtual device for assessing their presence in vegetables is gaining weight.
2. Analysis of published data and problem setting</p>
      <p>
        Organoleptic and sensory analysis are often used to assess food quality [
        <xref ref-type="bibr" rid="ref1">1</xref>
        ]. However, they cannot
be used to determine all the required quality characteristics with high accuracy. Measuring methods of
quality control allow for more accurate quality control of materials [
        <xref ref-type="bibr" rid="ref2">2</xref>
        ]. Depending on what processes
are the basis of the measurement method or what properties are used, measurement methods are
classified into: physical; chemical; physico-chemical; microbiological; technological; biochemical;
physiological (biological); commodity [
        <xref ref-type="bibr" rid="ref2">2</xref>
        ].
      </p>
      <p>However, measuring methods of food quality control have a number of disadvantages, in particular:
the long process of preparation of samples for measurement, the use of expensive instruments for
measurement, highly qualified specialists.</p>
      <p>
        According to the authors of the article, to study the quality of vegetables it is necessary to develop
methods that would have a wide range of uses, high sensitivity, resolution, easy sample preparation and
affordable and easy operation of the device in production conditions, significant analysis speed. Such
requirements are mainly met by conductometric research methods. The conductometric method is based
on measuring the electrical conductivity of objects of control. Currently, conductometry is used to
quickly determine the concentration of solutions of salts, acids, bases, to control the composition of
some industrial solutions. Preferably, these methods are used to control the individual quality indicators
of substances in the liquid state or gaseous medium [
        <xref ref-type="bibr" rid="ref3 ref4">3, 4</xref>
        ]. Conductometry includes direct methods of
analysis (used, for example, in salt meters) and indirect (for example, in gas analysis) using direct or
alternating current (low and high frequency), as well as chronoconductometry, low-frequency and
highfrequency titration [
        <xref ref-type="bibr" rid="ref5">5</xref>
        ]. Determination of the concentration is carried out by direct conductometry
(calibration schedule - allows you to directly determine the concentration of electrolyte by measuring
the conductivity of a solution with a known qualitative composition) or by conductometric titration
(analysis method based on determining the content of the substance by breaking the titration curve). ,
variable as a result of chemical reactions in the titration process). To determine the composition of the
liquid using the frequency dependence of the dielectric losses of the substance, as it is a characteristic
of the material. Conductometric analysis is based on changes in the concentration of a substance or
chemical composition of the medium in the interelectrode space; it is not related to the electrode
potential, which is often close to the equilibrium value. Indicators that characterize the non-electrical
properties of products are measured by converting the physico-chemical properties of substances and
materials into an electrical signal using various primary transducers (sensors) [
        <xref ref-type="bibr" rid="ref10 ref11 ref12 ref13 ref6 ref7 ref8 ref9">6-13</xref>
        ].
      </p>
      <p>
        The authors conducted experimental studies on the detection of heavy metals in vegetable juice and
obtained data reflecting physical parameters (complex stresses) proportional to the immittance. The
circuit consisted of a capacitive transducer (conductometric cell filled with model liquid - vegetable
juice with various impurities), RLC-meter to send a test signal to the capacitive transducer; block of
results processing and management [
        <xref ref-type="bibr" rid="ref14">14</xref>
        ].
      </p>
      <p>However, the above-described measurements performed using a standard RLC meter are limited by
the capabilities of the specified device in contrast to the virtual measuring instrument created using the
LabVIEW platform. The latter is considered optimal for providing software support for automated
control systems and research.</p>
    </sec>
    <sec id="sec-2">
      <title>3. The purpose and objectives of the study</title>
      <p>The purpose of this study is to improve the methodological and metrological support of quality
control of vegetables and their juices by studying the electrical parameters using a virtual means of
imitation control based on the hardware and computing platform LabVIEW.</p>
      <p>To achieve this goal should solve the following tasks:
 to develop a virtual tool for researching the quality of vegetable products on alternating current;
 to measure immittance by means of the NI USB 6009 block.</p>
      <p>The scientific novelty is the creation of a virtual device based on the LabVIEW platform, which
allows for operational research of grown vegetable products in-situ on alternating current. The virtual
instrument includes a test signal program and programs for processing the original voltage and current
of the object of study to calculate the immittance.</p>
      <p>Research methods. Theoretical bases of electrochemistry and qualimetry, measuring equipment,
programming are used, in particular within the LabVIEW hardware and computer platform. The
experiments were performed using modern measuring devices, including virtual ones, with automated
processing of measurement results. Studies have used a simulated method to measure the electrical
parameters of non-electrical objects, including vegetable juices.
4. Generation of test signal for imitation measurements</p>
      <p>
        The creation of a virtual device for monitoring the content of heavy metals (Cu, Pb, Zn) in vegetable
juice is based on the LabVIEW platform with the involvement of the NI USB 6009 unit [
        <xref ref-type="bibr" rid="ref15">15</xref>
        ]. The latter
is connected to a PC via a full-speed USB interface and has 8 channels of input analog signals (A1) to
generate and collect measured data; 12 digital I/O (DIO) channels and a 32-bit counter, as well as 2
analog signal generation (AO) channels, which perform the function of a test signal source (Figure 1).
      </p>
      <p>The LabVIEW graphics platform manages the NI USB 6009 using the NI-DAQ (National
Instruments - data acquisition) task. In the process of measurement the developed graphic software is
used: the program of a test signal and the program of processing of results of measurements.</p>
      <p>To measure and calculate the imitation of carrots generated a test signal - AC voltage with an
amplitude of 10-20 mV. To do this, perform the following steps:
1. Generation of a test signal (sine wave);
2. Reading of complex values of immittance.</p>
      <p>NI USB 6009
Virtual tool</p>
      <sec id="sec-2-1">
        <title>LabVIEW</title>
        <p>DTS</p>
        <p>Ux, Ix</p>
        <p>Conductometric cell</p>
        <p>The NI USB 6009 unit is designed to generate a DC voltage of 5 V at a maximum current of 5 mA.
According to the immittance measurement technique, the test signal is a sine wave. Because this unit
does not generate AC voltage, the program used individual elements of the NI-DAQ task and the While
Loop with Stop Button loop. In addition, the program records the Wait command, which specifies the
interval between iterations of the loop. The number of sinusoidal points is set on the Points per cycle
indicator (Figure 2-3).</p>
        <p>The created device allows to generate electric voltage in the range 0… 5 V. At the same time, the
program deduces a sinusoidal signal with voltage shift and allows the user to choose the number of
points per cycle. Increasing the dots per cycle increases the resolution of the output signal, but decreases
its frequency. The approximation period of the output signal is equal to the number of points per cycle
multiplied by the time norm (Figure 2-3).
1. Open Test signal NI USB-6009 VI.
2. Adjust the front (front) panel controls: Physical channel; Maximum value; Minimum value;
Output speed; Number of points per cycle.
3. Run the Test signal NI USB-6009 VI (Figure 2).</p>
        <p>All steps are performed in the LabVIEW software package. The obtained experimental data are
processed using the tools of the graphics platform LabVIEW.</p>
        <p>The virtual device for measuring the immittance of non-electric objects has: PC with installed
software, NI USB 6009 unit, which is used to generate a sinusoidal signal and apply it to a container
with graphite electrodes filled with juice or modeling solution. The same unit is used to measure
immittance.
5. Measurement of immittance by means of the NI USB 6009 block</p>
        <p>A typical immittance measurement requires one transducer to measure the voltage at the load
terminals and a second transducer to measure the current flowing through the object. However, the
actual calculation of the immittance depends on the resistive and reactive components (capacitors and
/ or inductors) in the circuit. Reactive components lead to a phase shift (up to 90 degrees) between
voltage and current signals. This phenomenon is represented by three different representations of
imitance: the active component, the module and the reactive component. These three components have
phase connections that can be visualized in the immittance triangle shown in Figure 4.</p>
        <p>There are various methods used to measure the active impedance component. The first method is to
take the average time value of the instantaneous product of voltage and current to calculate the active
power and then divide it by the square of the current value. Another way is to use the impedance angle
depicted in the immittance triangle. The cosine of the impedance angle, directly proportional to the
active resistance in the circuit, is called the impedance coefficient.</p>
        <p>
          Immittance measurement through complex power. Reactive components cause a phase shift (up to
90 degrees) between voltage and current. Current and voltage signals have a phase shift in the range of
0 and 90 degrees. To measure the reactive component, the following capabilities are required: the ability
to obtain a voltage and current signal; simultaneous receipt of both measuring signals; both measuring
instruments must receive signals simultaneously. The LabVIEW software and hardware platform
includes a number of virtual devices that work with DAQ hardware devices. For a single-phase circuit,
the voltage and current signals have the following expressions:
 ( ) =  √2 , (1)
 ( ) =  √2sin( −  ). (2)
Ratio - active power relative to the square of the current value [
          <xref ref-type="bibr" rid="ref16">16</xref>
          ]:
 =
∫
( )∗ ( )
.
        </p>
        <p>(3)</p>
        <p>= | | sin 
Reactive component
j
|Z|
| | = √
+ 
=</p>
        <p>⁄</p>
      </sec>
      <sec id="sec-2-2">
        <title>Resistance module</title>
        <p>Z = R + jX</p>
      </sec>
      <sec id="sec-2-3">
        <title>Complex resistance</title>
        <p>θ</p>
        <p>R</p>
        <p>= | | cos</p>
      </sec>
      <sec id="sec-2-4">
        <title>Active component</title>
      </sec>
      <sec id="sec-2-5">
        <title>Real</title>
        <p>
          This operation of calculating the specified ratio requires two operations, namely to multiply the
instantaneous values of current and voltage; calculate and give the result of indirect measurement and
divide it by the square of the current value. The modulus of complex resistance, | Z |, which is defined
as the division of the root mean square (current) values of voltage and current, is obtained by the ratio
[
          <xref ref-type="bibr" rid="ref16">16</xref>
          ]:
other for current.
        </p>
        <p>Taking into account these connections, two measuring contacts are defined: one for voltage and the
To calculate the RMS values of voltage and current used virtual instruments, which are in the
subpalette of functions "VI Express" Signal analysis, by dividing the RMS values of voltage and
current, the modulus of impedance Z is obtained (Figure 5).
| | =  с/Іс.</p>
        <p>By multiplying the instantaneous values of voltage and current and passing through a low-pass filter
(Express Filter VI), we obtain the active power, and then the active component R (Figure 6).</p>
        <p>The reactive component is determined by the ratio:
 = √
−  .</p>
        <p>(4)
(5)
The device (Figure 5-7) used:
 Filter to obtain the integral of the product of the voltage and current values of the object of
study;
 MEAN to calculate the average value for the period at the output of the filter;
 Amplitude and Level Measurement to obtain the current value;
 DAQ Assistant to obtain the original voltage and current values of the object of study.</p>
        <p>The window for setting the amplitude measurements is shown in Figure 8.</p>
        <p>This analysis of the measured values of voltage and current is used to calculate the modulus of
admittance. The RMS option is selected in this window. The output is the root mean square value of
the voltage or current signal.</p>
        <p>The window for setting the electric filter is shown in Figure 9.</p>
        <p>The design of the virtual filter in the composition: the filter, the RMS meter and the average value
at the output of the filter, is used to calculate the active component of the impedance. In the window
you can select the filter settings, operating frequency range, etc.</p>
        <p>
          Calculation of immittance using the Euler equation. To represent voltage and current signals with
complex values, we use the laws of electrical engineering [
          <xref ref-type="bibr" rid="ref16">16</xref>
          ]. Yes, AC voltage or current:
are as follows:
        </p>
        <p>Using Euler's equation:
i=Im sin(ωt+φi),
u=Um sin(ωt+φu),
 =  cos(
 ̇ =   cos 
+  ) +  ∗  sin(
+   +  ∗   sin(
+  ),</p>
        <p>+   ).
 =   ( ),
 ̇ =     ( +  ),
write the impedance of the measuring object:
( )
 = ( ) . (12)</p>
        <p>
          Therefore, to measure the impedance, it is necessary to measure the amplitudes and phases of the
voltage and current signals [
          <xref ref-type="bibr" rid="ref16">16</xref>
          ]. The window for adjusting the measurement of the amplitude and phase
of the measuring signals of voltage and current is shown in Figure 10.
(6)
(7)
(8)
(9)
(10)
(11)
In the created device (Figure 11) are used:
 Tone Measurement – to obtain the amplitude and phase of the measured values of voltage and
current;
 DAQ Assistant - to obtain the original values of voltage and current of the object of study;
 Adapter for converting measurement data to numeric;
 Elements of transformation of complex numbers.
        </p>
      </sec>
    </sec>
    <sec id="sec-3">
      <title>6. Conclusions</title>
      <p>For imitative control of vegetable juice quality indicators, a virtual measuring instrument based on
the hardware and software platform LabVIEW and a compatible NI USB 6009 unit has been proposed,
developed and implemented.</p>
      <p>A sinusoidal test signal in the form of an alternating voltage with an amplitude of 10-20 mV was
generated to measure and calculate the imitance of the object. Because the NI USB 6009 unit is not able
to generate AC voltage, the program uses some elements of the NI-DAQ task with the While Loop with
Stop Button cycle. To do this, create a generation channel Create Channel (start generation Start, write
voltage generation, clear task Clear Task), as well as Wait, which regulates the sine wave period.</p>
      <p>Reading and processing of complex components of imitation is carried out in 2 ways:
 Using Euler's equation;
 By module and active immittance component (Amplitude &amp; Level measurement → RMS (root
mean square) was used to obtain the immittance module value, and Filter i mean was used to obtain
the active immittance component). In this case, the reactive component of immittance is calculated
algebraically.</p>
      <p>A structure has been developed that allows switching to the desired type of measurement, based on
the recorded instantaneous values of voltage and current of the conductometric cell, ie on SCR voltage
measurements, SCR current measurements, module measurements, measurements of active and
reactive components.
7. References</p>
    </sec>
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